Synthesis of nitrogen and sulfur co-doped yolk-shell porous carbon microspheres and their application for Pb(II) detection in fish serum
Wang, HQ (Wang, Haoqiang)[ 1 ]; Xu, RY (Xu, Ruiyu)[ 2,3,4 ]; Chen, H (Chen, Han)[ 1 ]; Yuan, QH (Yuan, Qunhui)[ 1,2,3 ]
2018
Source PublicationJOURNAL OF SOLID STATE CHEMISTRY
ISSN0022-4596
Volume266Issue:10Pages:63-69
Abstract

Nitrogen (N) and sulfur (S) co-doped carbonaceous material has shown remarkably improved performance in electrocatalysis, supercapacitor, and so on. While, the application of N, S co-doped carbon in electrochemical sensor was less investigated. Herein, N, S co-doped yolk-shell porous carbon microspheres (N, S-YSPCMSs) were synthesized by silica templating strategy and high-temperature pyrolysis method. The as-prepared N, S-YSPCMSs exhibited spherical morphologies, porous structures and high N, S-doping contents. Owing to the synergetic effect of the well-dispersed N,S-dopants, good conductivity of carbon skeleton, high surface area and pore volume of the microspheres, the N, S-YSPCMSs prepared at 900 degrees C showed good electrochemical performance for Pb(II) and with a linear range of 4-160 mu g L-1, the limit of detection is 0.49 mu g L-1 (S/N = 3). The electrochemical sensor was consequently applied in detecting Pb(II) in fish serum samples with satisfying recoveries, indicating the N, S-YSPCMSs-900 are promising electrode components for electroanalysis.

Keywordn, s Co-doped Porous Carbon Microspheres Electrochemical Sensor Lead Ion Differential Pulse Anodic Stripping Voltammetry Fish Serum
DOI10.1016/j.jssc.2018.07.002
Indexed BySCI
CSCD IDCSCD:000444664800009
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Document Type期刊论文
Identifierhttp://ir.xjipc.cas.cn/handle/365002/5591
Collection中国科学院特殊环境功能材料与器件重点试验室
Affiliation1.Harbin Inst Technol Shenzhen, Sch Mat Sci & Engn, Shenzhen 518055, Peoples R China
2.Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Lab Environm Sci & Technol, Urumqi 830011, Peoples R China
3.Chinese Acad Sci, Key Lab Funct Mat & Devices Special Environm, Urumqi 830011, Peoples R China
4.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
Recommended Citation
GB/T 7714
Wang, HQ ,Xu, RY ,Chen, H ,et al. Synthesis of nitrogen and sulfur co-doped yolk-shell porous carbon microspheres and their application for Pb(II) detection in fish serum[J]. JOURNAL OF SOLID STATE CHEMISTRY,2018,266(10):63-69.
APA Wang, HQ ,Xu, RY ,Chen, H ,&Yuan, QH .(2018).Synthesis of nitrogen and sulfur co-doped yolk-shell porous carbon microspheres and their application for Pb(II) detection in fish serum.JOURNAL OF SOLID STATE CHEMISTRY,266(10),63-69.
MLA Wang, HQ ,et al."Synthesis of nitrogen and sulfur co-doped yolk-shell porous carbon microspheres and their application for Pb(II) detection in fish serum".JOURNAL OF SOLID STATE CHEMISTRY 266.10(2018):63-69.
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