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N-Doped Hollow Porous Carbon Spheres/Bismuth Hybrid Film Modified Electrodes for Sensitive Voltammetric Determination of Trace Cadmium
Qin, DF (Qin, Danfeng)[ 1 ]; Wang, L (Wang, Le)[ 1 ]; Gao, SS (Gao, Sanshuang)[ 1 ]; Wang, Y (Wang, Ying)[ 1,4 ]; Mamat, X (Mamat, Xamxikamar)[ 1 ]; Li, YT (Li, Yongtao)[ 1 ]; Wagberg, T (Wagberg, Thomas)[ 2 ]; Cheng, H (Cheng, Hao)[ 3 ]; Hu, GZ (Hu, Guangzhi)[ 1,2 ]
2018
Source PublicationELECTROANALYSIS
ISSN1040-0397
Volume30Issue:9Pages:1906-1912
Abstract

In this work, N-doped hollow porous carbon spheres (N-HPCSs) were synthesized by silicon dioxide template-assisted polybenzoxazine (PB) coating strategy. The prepared N-HPCSs have a smooth hollow ball structure surrounded by a well-defined porous shell. Combining with in-situ plating of Bi film, the N-HPCSs were further fabricated a sensitive electrochemical platform for determination trace levels of Cd(II) by differential pulse anodic stripping voltammetry (DPASV). Under the optimized conditions, the Bi-N-HPCSs based sensor displays a linear response to Cd(II) over the range of 0.5gL(-1) to 150gL(-1). Meanwhile, the limit of detection (LOD, S/N=3) is estimated to be around 0.16gL(-1) for Cd(II), which is 31 times lower than the safety values set by United States Environmental Protection Agency (EPA) for the drinking water. Moreover, the proposed method was successfully applied to detection of Cd(II) in tap water and lake water, and the analytical results of the presented method are agreed well with inductively coupled plasma-mass spectrometry (ICP-MS) data. Due to the excellent analytical performance, the fabricated electrode is promised for future development in monitoring of cadmium pollution in the environment.

KeywordN-doped Hollow Porous Carbon Spheres Bismuth Film Differential Pulse Anodic Stripping Voltammetry Cadmium Tap Water Lake Water
DOI10.1002/elan.201700839
Indexed BySCI
WOS IDWOS:000443938300004
Citation statistics
Cited Times:2[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.xjipc.cas.cn/handle/365002/5579
Collection省部共建新疆特有药用资源利用重点实验室
Corresponding AuthorMamat, X (Mamat, Xamxikamar)[ 1 ]; Hu, GZ (Hu, Guangzhi)[ 1,2 ]
Affiliation1.Chinese Acad Sci, Key Lab Chem Plant Resources Arid Reg, State Key Lab Basis Xinjiang Indigenous Med Plant, Xinjiang Tech Inst Phys & Chem, Urumqi 830011, Peoples R China
2.Umea Univ, Dept Phys, S-90187 Umea, Sweden
3.Guangxi Univ Sci & Technol, Guangxi Key Lab Green Proc Sugar Resources, Liuzhou 545006, Peoples R China
4.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
Recommended Citation
GB/T 7714
Qin, DF ,Wang, L ,Gao, SS ,et al. N-Doped Hollow Porous Carbon Spheres/Bismuth Hybrid Film Modified Electrodes for Sensitive Voltammetric Determination of Trace Cadmium[J]. ELECTROANALYSIS,2018,30(9):1906-1912.
APA Qin, DF .,Wang, L .,Gao, SS .,Wang, Y .,Mamat, X .,...&Hu, GZ .(2018).N-Doped Hollow Porous Carbon Spheres/Bismuth Hybrid Film Modified Electrodes for Sensitive Voltammetric Determination of Trace Cadmium.ELECTROANALYSIS,30(9),1906-1912.
MLA Qin, DF ,et al."N-Doped Hollow Porous Carbon Spheres/Bismuth Hybrid Film Modified Electrodes for Sensitive Voltammetric Determination of Trace Cadmium".ELECTROANALYSIS 30.9(2018):1906-1912.
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