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Engineering studies on the direct synthesis of methyl chlorosilane in fluidized bed reactor with multiple tubular and segmented heat transfer
Wang, Q (Wang Qiang)[ 1,2 ]; Zhang, ZW (Zhang Zhengwei)[ 1 ]; Wang, X (Wang Xu)[ 1 ]; Gao, L (Gao Lin)[ 1 ]
2018
发表期刊PRZEMYSL CHEMICZNY
ISSN0033-2496
卷号97期号:7页码:1144-1150
摘要

The fluidized bed reactor with multiple tubular and segmented heat transfer was employed to study the effects of mass flow rate of MeCl and reaction pressure on the rate of MeCl conversion and the methyl chlorosilane yield at 300 degrees C. The rate of MeCl conversion and the yield of Me2SiCl2 were not always increased with increasing mass flow rate of MeCl at constant reaction pressure under particular operating conditions. At constant mass flow rate, the rate of MeCl conversion and the yield of Me2SiCl2 decreased first, and then increased with increasing reaction pressure. Therefore, for the fluidized bed reaction system, a synergism between the MeCl mass flow and reaction pressure in effecting the MeCl conversion rate and the yield of Me2SiCl2 was obsd. The reaction pressure for optimum yield of Me2SiCl2 was 0.30 MPa and MeCl mass flow rate was 4.5 kg/h.

DOI10.15199/62.2018.7.22
收录类别SCI
WOS记录号WOS:000443795000025
引用统计
文献类型期刊论文
条目标识符http://ir.xjipc.cas.cn/handle/365002/5573
专题资源化学研究室
通讯作者Wang, Q (Wang Qiang)[ 1,2 ]
作者单位1.Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Urumqi 830011, Peoples R China
2.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
推荐引用方式
GB/T 7714
Wang, Q ,Zhang, ZW ,Wang, X ,et al. Engineering studies on the direct synthesis of methyl chlorosilane in fluidized bed reactor with multiple tubular and segmented heat transfer[J]. PRZEMYSL CHEMICZNY,2018,97(7):1144-1150.
APA Wang, Q ,Zhang, ZW ,Wang, X ,&Gao, L .(2018).Engineering studies on the direct synthesis of methyl chlorosilane in fluidized bed reactor with multiple tubular and segmented heat transfer.PRZEMYSL CHEMICZNY,97(7),1144-1150.
MLA Wang, Q ,et al."Engineering studies on the direct synthesis of methyl chlorosilane in fluidized bed reactor with multiple tubular and segmented heat transfer".PRZEMYSL CHEMICZNY 97.7(2018):1144-1150.
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