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Engineering studies on the direct synthesis of methyl chlorosilane in fluidized bed reactor with multiple tubular and segmented heat transfer
Wang, Q (Wang Qiang)[ 1,2 ]; Zhang, ZW (Zhang Zhengwei)[ 1 ]; Wang, X (Wang Xu)[ 1 ]; Gao, L (Gao Lin)[ 1 ]
2018
Source PublicationPRZEMYSL CHEMICZNY
ISSN0033-2496
Volume97Issue:7Pages:1144-1150
Abstract

The fluidized bed reactor with multiple tubular and segmented heat transfer was employed to study the effects of mass flow rate of MeCl and reaction pressure on the rate of MeCl conversion and the methyl chlorosilane yield at 300 degrees C. The rate of MeCl conversion and the yield of Me2SiCl2 were not always increased with increasing mass flow rate of MeCl at constant reaction pressure under particular operating conditions. At constant mass flow rate, the rate of MeCl conversion and the yield of Me2SiCl2 decreased first, and then increased with increasing reaction pressure. Therefore, for the fluidized bed reaction system, a synergism between the MeCl mass flow and reaction pressure in effecting the MeCl conversion rate and the yield of Me2SiCl2 was obsd. The reaction pressure for optimum yield of Me2SiCl2 was 0.30 MPa and MeCl mass flow rate was 4.5 kg/h.

DOI10.15199/62.2018.7.22
Indexed BySCI
WOS IDWOS:000443795000025
Citation statistics
Document Type期刊论文
Identifierhttp://ir.xjipc.cas.cn/handle/365002/5573
Collection资源化学研究室
Corresponding AuthorWang, Q (Wang Qiang)[ 1,2 ]
Affiliation1.Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Urumqi 830011, Peoples R China
2.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
Recommended Citation
GB/T 7714
Wang, Q ,Zhang, ZW ,Wang, X ,et al. Engineering studies on the direct synthesis of methyl chlorosilane in fluidized bed reactor with multiple tubular and segmented heat transfer[J]. PRZEMYSL CHEMICZNY,2018,97(7):1144-1150.
APA Wang, Q ,Zhang, ZW ,Wang, X ,&Gao, L .(2018).Engineering studies on the direct synthesis of methyl chlorosilane in fluidized bed reactor with multiple tubular and segmented heat transfer.PRZEMYSL CHEMICZNY,97(7),1144-1150.
MLA Wang, Q ,et al."Engineering studies on the direct synthesis of methyl chlorosilane in fluidized bed reactor with multiple tubular and segmented heat transfer".PRZEMYSL CHEMICZNY 97.7(2018):1144-1150.
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