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HPLC法同时测定新疆贝母中3种核苷类成分
艾则孜·莫合买提; 沙丽娜; 单莲莲; 阿布力米提·伊力
2017
Source Publication中成药
ISSN1001-1528
Volume39Issue:5Pages:1097-1099
Abstract

目的建立HPLC法同时测定新疆贝母中3种核苷类成分的含有量。方法贝母水提液的分析采用Waters Sun Fire TM-C18色谱柱(4.6 mm×150 mm,5μm);流动相甲醇-水(10∶90),等度洗脱;体积流量0.8 m L/min;柱温25℃;检测波长260 nm。结果尿苷、胸苷、腺苷分别在10.04501.93μg/m L(r=0.997 5)、0.105.07μg/m L(r=0.999 8)、1.0150.39μg/m L(r=0.999 9)范围内呈良好的线性关系,平均加样回收率分别为103.11%(RSD=1.45%)、99.33%(RSD=1.68%)、98.25%(RSD=1.57%)。结论该方法简便准确,灵敏度高,专属性好,可用于新疆贝母的质量控制。

Keyword新疆贝母 尿苷 胸苷 腺苷 Hplc
Indexed ByCSCD
CSCD IDCSCD:5981889
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Document Type期刊论文
Identifierhttp://ir.xjipc.cas.cn/handle/365002/4811
Collection资源化学研究室
Affiliation中国科学院新疆理化技术研究所;中国科学院研究生院;新疆维吾尔自治区食品药品检验所
Recommended Citation
GB/T 7714
艾则孜·莫合买提,沙丽娜,单莲莲,等. HPLC法同时测定新疆贝母中3种核苷类成分[J]. 中成药,2017,39(5):1097-1099.
APA 艾则孜·莫合买提,沙丽娜,单莲莲,&阿布力米提·伊力.(2017).HPLC法同时测定新疆贝母中3种核苷类成分.中成药,39(5),1097-1099.
MLA 艾则孜·莫合买提,et al."HPLC法同时测定新疆贝母中3种核苷类成分".中成药 39.5(2017):1097-1099.
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