Chemical Fingerprint Analysis and Quantitative Analysis of Rosa rugosa by UPLC-DAD
Mansur, S (Mansur, Sanawar); Abdulla, R (Abdulla, Rahima); Ayupbec, A (Ayupbec, Amatjan); Aisa, HA (Aisa, Haji Akbar); Aisa, HA
2016
发表期刊MOLECULES
卷号21期号:2
摘要A method based on ultra performance liquid chromatography with a diode array detector (UPLC-DAD) was developed for quantitative analysis of five active compounds and chemical fingerprint analysis of Rosa rugosa. Ten batches of R. rugosa collected from different plantations in the Xinjiang region of China were used to establish the fingerprint. The feasibility and advantages of the used UPLC fingerprint were verified for its similarity evaluation by systematically comparing chromatograms with professional analytical software recommended by State Food and Drug Administration (SFDA) of China. In quantitative analysis, the five compounds showed good regression (R-2 = 0.9995) within the test ranges, and the recovery of the method was in the range of 94.2%-103.8%. The similarities of liquid chromatography fingerprints of 10 batches of R. rugosa were more than 0.981. The developed UPLC fingerprint method is simple, reliable, and validated for the quality control and identification of R. rugosa. Additionally, simultaneous quantification of five major bioactive ingredients in the R. rugosa samples was conducted to interpret the consistency of the quality test. The results indicated that the UPLC fingerprint, as a characteristic distinguishing method combining similarity evaluation and quantification analysis, can be successfully used to assess the quality and to identify the authenticity of R. rugosa.
关键词Rosa Rugosa Uplc-dad Quality Control Fingerprint
DOI10.3390/molecules21121754
收录类别SCI
WOS记录号WOS:000392140100148
引用统计
被引频次:2[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.xjipc.cas.cn/handle/365002/4715
专题省部共建新疆特有药用资源利用重点实验室
通讯作者Aisa, HA
作者单位1.Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Key Lab Xinjiang Indigenous Med Plants Resource U, Urumqi 830011, Peoples R China
2.Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Key Lab Plant Resources & Chem Arid Reg, Urumqi 830011, Peoples R China
3.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
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Mansur, S ,Abdulla, R ,Ayupbec, A ,et al. Chemical Fingerprint Analysis and Quantitative Analysis of Rosa rugosa by UPLC-DAD[J]. MOLECULES,2016,21(2).
APA Mansur, S ,Abdulla, R ,Ayupbec, A ,Aisa, HA ,&Aisa, HA.(2016).Chemical Fingerprint Analysis and Quantitative Analysis of Rosa rugosa by UPLC-DAD.MOLECULES,21(2).
MLA Mansur, S ,et al."Chemical Fingerprint Analysis and Quantitative Analysis of Rosa rugosa by UPLC-DAD".MOLECULES 21.2(2016).
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