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题名: Synthesis and characterization of Mn-Co-Ni-O ceramic nanoparticles by reverse microemulsion method
作者: Chen, L (Chen, Long); Kong, WW (Kong, Wenwen); Yao, JC (Yao, Jincheng); Zhang, HH (Zhang, Huhnin); Gao, B (Gao, Bo); Li, YL (Li, Yonglei); Bu, HJ (Bu, Haijun); Chang, AM (Chang, Aimin); Jiang, CP (Jiang, Chunping)
通讯作者: Chang, AM
关键词: Mn-Co-Ni-O nanoparticles ; Reverse microemulsion method ; Calcination temperature
刊名: CERAMICS INTERNATIONAL
发表日期: 2015
DOI: 10.1016/j.ceramint.2014.10.106
卷: 41, 期:2, 页:2847-2851
收录类别: SCI
资助者: Chinese Academy of SciencesNational High Technology Research and Development Program of China;Chinese Academy of SciencesTalent Program of Xinjiang Uygur Autonomous Region;
摘要: Mn-Co-Ni-O ultrafine ceramic nanoparticles are successfully synthesized by the reverse microemulsion method in a triton X-100/n-hexanol/cyclohexane system. The thermal decomposition process, crystallinity and crystal structure of Mn-Co-Ni-O powders are investigated and characterized by thermogravimetric-differential scanning calorimetry (TG/DSC), Fourier Transform Infrared (FT-IR), X-ray powders diffraction (XRD) and High Resolution Transmission Electron Microscope (HRTEM), respectively. The TGA/DSC, FT-IR and XRD results show that the reverse microemulsion method can effectively reduce the calcination temperature to 600 degrees C for synthesizing cubic spinel phase Mn-Co-Ni-O ceramic particles. Furthermore, the XRD and HRTEM images reveal that the particles are highly crystalline and have a narrow and uniform particle size distribution. These findings indicate that Mn-Co-Ni-O nanoparticles prepared via reverse microemulsion process meet demands for obtaining better microstructure and performance of Mn-Co-Ni-O materials.
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内容类型: 期刊论文
URI标识: http://ir.xjipc.cas.cn/handle/365002/4202
Appears in Collections:中国科学院特殊环境功能材料与器件重点试验室_期刊论文

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作者单位: Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Key Lab Funct Mat & Devices Special Environm, Key Lab Elect Informat Mat & Devices, Urumqi 830011, Xinjiang, Peoples R China;Univ Chinese Acad Sci, Beijing 100049, Peoples R China;Chinese Acad Sci, Key Lab Nanodevices & Applicat, Suzhou Inst Nanotech & Nanob, Suzhou 215123, Peoples R China

Recommended Citation:
Chen, L ,Kong, WW ,Yao, JC ,et al. Synthesis and characterization of Mn-Co-Ni-O ceramic nanoparticles by reverse microemulsion method[J]. CERAMICS INTERNATIONAL,2015,41(2):2847-2851.
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