Synthesis and characterization of Mn-Co-Ni-O ceramic nanoparticles by reverse microemulsion method
Chen, L (Chen, Long); Kong, WW (Kong, Wenwen); Yao, JC (Yao, Jincheng); Zhang, HH (Zhang, Huhnin); Gao, B (Gao, Bo); Li, YL (Li, Yonglei); Bu, HJ (Bu, Haijun); Chang, AM (Chang, Aimin); Jiang, CP (Jiang, Chunping)
2015
Source PublicationCERAMICS INTERNATIONAL
ISSN0272-8842
Volume41Issue:2Pages:2847-2851
Abstract

Mn-Co-Ni-O ultrafine ceramic nanoparticles are successfully synthesized by the reverse microemulsion method in a triton X-100/n-hexanol/cyclohexane system. The thermal decomposition process, crystallinity and crystal structure of Mn-Co-Ni-O powders are investigated and characterized by thermogravimetric-differential scanning calorimetry (TG/DSC), Fourier Transform Infrared (FT-IR), X-ray powders diffraction (XRD) and High Resolution Transmission Electron Microscope (HRTEM), respectively. The TGA/DSC, FT-IR and XRD results show that the reverse microemulsion method can effectively reduce the calcination temperature to 600 degrees C for synthesizing cubic spinel phase Mn-Co-Ni-O ceramic particles. Furthermore, the XRD and HRTEM images reveal that the particles are highly crystalline and have a narrow and uniform particle size distribution. These findings indicate that Mn-Co-Ni-O nanoparticles prepared via reverse microemulsion process meet demands for obtaining better microstructure and performance of Mn-Co-Ni-O materials.

KeywordMn-co-ni-o Nanoparticles Reverse Microemulsion Method Calcination Temperature
DOI10.1016/j.ceramint.2014.10.106
Indexed BySCI
WOS IDWOS:000348003100027
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Cited Times:14[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.xjipc.cas.cn/handle/365002/4202
Collection中国科学院特殊环境功能材料与器件重点试验室
材料物理与化学研究室
Affiliation1.Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Key Lab Funct Mat & Devices Special Environm, Key Lab Elect Informat Mat & Devices, Urumqi 830011, Xinjiang, Peoples R China
2.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
3.Chinese Acad Sci, Key Lab Nanodevices & Applicat, Suzhou Inst Nanotech & Nanob, Suzhou 215123, Peoples R China
Recommended Citation
GB/T 7714
Chen, L ,Kong, WW ,Yao, JC ,et al. Synthesis and characterization of Mn-Co-Ni-O ceramic nanoparticles by reverse microemulsion method[J]. CERAMICS INTERNATIONAL,2015,41(2):2847-2851.
APA Chen, L .,Kong, WW .,Yao, JC .,Zhang, HH .,Gao, B .,...&Jiang, CP .(2015).Synthesis and characterization of Mn-Co-Ni-O ceramic nanoparticles by reverse microemulsion method.CERAMICS INTERNATIONAL,41(2),2847-2851.
MLA Chen, L ,et al."Synthesis and characterization of Mn-Co-Ni-O ceramic nanoparticles by reverse microemulsion method".CERAMICS INTERNATIONAL 41.2(2015):2847-2851.
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