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Synthesis of LiCo1/3Ni1/3Mn1/3O(2) as a layered cathode material prepared by the Pechini process
Li, Zhigang; Kang, Xueya; Wang, Tiandiao; Han, Ying
2006
发表期刊MATERIALS TECHNOLOGY
ISSN1066-7857
卷号21期号:4页码:229-232
摘要

In a study, a layered LiCO1/ 3Mn1/3Ni1/ 3O2 include a solid-state solution method, co-precipitation, mixed hydroxide method, layered double hydroxides solid state reaction, spray dry method and the metal ecetate decomposition method. In the study, layered LiCO1/ 3Mn1/ 3Ni1/ 3O2 was first prepared by the Pechini process. Ni(NO3)2·6H2O(AR), Co(NO3)2·6H2O(AR) and Mn(NO3)2(AR) were mixed and dissolved in deionized water in a molar ration of Ni/Co/Mn =1:1:1. The aqueous solution was slowly dripped into a mixed solution of NH3·H2O and NaOH at a constant rate. The stoichiometric starting materials NiO(AR), Co(NO3)2·6H2O(AR) and Mn(CH3COO)2·H2O(AR) were dispersed in acetone and mixed. The structure and morphology of the prepared powders was characterized using Xray difraction and scanning electron microscopy. Results show that Sample 1 had a phase pure a-NaFeO2 structure and the least ion mixing degree in the lattice with fine, uniform particle sizes. They developed a well layered structure and are anticipated to display an excellent electrochemical performance. The new approach requires only low temperatures and saves on energy consumption.

DOI10.1179/mte.2006.21.4.229
收录类别SCI
WOS记录号WOS:000243582100006
引用统计
文献类型期刊论文
条目标识符http://ir.xjipc.cas.cn/handle/365002/4126
专题材料物理与化学研究室
作者单位Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China;Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Urumuqi Xinjiang 830011, Peoples R China
推荐引用方式
GB/T 7714
Li, Zhigang,Kang, Xueya,Wang, Tiandiao,et al. Synthesis of LiCo1/3Ni1/3Mn1/3O(2) as a layered cathode material prepared by the Pechini process[J]. MATERIALS TECHNOLOGY,2006,21(4):229-232.
APA Li, Zhigang,Kang, Xueya,Wang, Tiandiao,&Han, Ying.(2006).Synthesis of LiCo1/3Ni1/3Mn1/3O(2) as a layered cathode material prepared by the Pechini process.MATERIALS TECHNOLOGY,21(4),229-232.
MLA Li, Zhigang,et al."Synthesis of LiCo1/3Ni1/3Mn1/3O(2) as a layered cathode material prepared by the Pechini process".MATERIALS TECHNOLOGY 21.4(2006):229-232.
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