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题名: Synthesis, structure, and properties of Li2Pb2CuB4O10 with isolated [CuB4O10](6-) units
作者: Li, Hongyi; Pan, Shilie; Wu, Hongping; Smit, Jared P.; Poeppelmeier, Kenneth R.
通讯作者: Pan, SL
关键词: Oxide materials ; Solid state reactions ; Crystal structure ; X-ray diffraction
刊名: Journal of Alloys and Compounds
发表日期: 2011
DOI: 10.1016/j.jallcom.2010.11.206
卷: 509, 期:7, 页:3310-3313
收录类别: SCI ; EI
摘要: The copper borate Li2Pb2CuB4O10 has been synthesized in air by the standard solid-state reaction at temperature in the range 550-650 °C and the structure of Li2Pb 2CuB4O10 was determined by single-crystal X-ray diffraction. Li2Pb2CuB4O10 crystallizes in the monoclinic space group C2/c (no. 15) with a = 16.8419(12), b = 4.7895(4), c = 13.8976(10) , and β = 125.3620(10)°, V = 914.22(12) 3, and Z = 4, as determined by single-crystal X-ray diffraction. The Li2Pb2CuB4O10 structure exhibits isolated units of stoichiometry [CuB4O10]6- that are built from CuO4 distorted square planes and triangular BO3 groups. The IR spectroscopy and thermal analysis investigations of Li2Pb2CuB4O10 are also presented.
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内容类型: 期刊论文
URI标识: http://ir.xjipc.cas.cn/handle/365002/4029
Appears in Collections:新疆维吾尔自治区电子信息材料与器件重点实验室_期刊论文

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作者单位: Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Xinjiang Key Lab Elect Informat Mat & Devices, Urumqi 830011, Peoples R China;Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China; Northwestern Univ, Dept Chem, Evanston, IL 60208 USA

Recommended Citation:
Li, Hongyi,Pan, Shilie,Wu, Hongping,et al. Synthesis, structure, and properties of Li2Pb2CuB4O10 with isolated [CuB4O10](6-) units[J]. Journal of Alloys and Compounds,2011,509(7):3310-3313.
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