A new polymorph of Cd3B2O6: synthesis, crystal structure and phase transformation
Zhang, Xingwen; Yu, Hongwei; Wu, Hongping; Pan, Shilie; Jiao, Anqing; Zhang, Bingbing; Yang, Zhihua
2014
Source PublicationRSC Advances
ISSN2046-2069
Volume4Issue:25Pages:13195-13200
Abstract

A new polymorph of Cd3B2O6 (β-Cd 3B2O6) has been grown through spontaneous crystallization with the flux system. β-Cd3B2O 6 crystallizes in triclinic space group P1 and features a three-dimensional Cd-O network composed of CdOn (n = 5, 6) distorted polyhedra and isolated planar BO3 groups. The phase transformation of Cd3B2O6 has been studied by the structure analysis and powder X-ray diffraction. TG-DSC measurement reveals the melting behavior and phase transformation temperature. Furthermore, the IR spectrum was measured. The detailed structure comparison between Cd3B 2O6 and other cadmium-containing borates, such as CdB 4O7, CdB2O4 and Cd2B 2O5 was also carried out.

DOI10.1039/c4ra00671b
Indexed BySCI
WOS IDWOS:000332485000070
Citation statistics
Cited Times:12[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.xjipc.cas.cn/handle/365002/3833
Collection中国科学院特殊环境功能材料与器件重点试验室
材料物理与化学研究室
Affiliation1.Xinjiang Tech Inst Phys & Chem CAS, Xinjiang Key Lab Elect Informat Mat & Devices, Key Lab Funct Mat & Devices Special Environm CAS, Urumqi 830011, Peoples R China
2.Univ Chinese Acad Sci, Beijing 100049, Peoples R China
Recommended Citation
GB/T 7714
Zhang, Xingwen,Yu, Hongwei,Wu, Hongping,et al. A new polymorph of Cd3B2O6: synthesis, crystal structure and phase transformation[J]. RSC Advances,2014,4(25):13195-13200.
APA Zhang, Xingwen.,Yu, Hongwei.,Wu, Hongping.,Pan, Shilie.,Jiao, Anqing.,...&Yang, Zhihua.(2014).A new polymorph of Cd3B2O6: synthesis, crystal structure and phase transformation.RSC Advances,4(25),13195-13200.
MLA Zhang, Xingwen,et al."A new polymorph of Cd3B2O6: synthesis, crystal structure and phase transformation".RSC Advances 4.25(2014):13195-13200.
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