一种用微波反应制备壬二酸的方法
吾满江.艾力; 高军军; 张亚刚; 董昕; 胡书明; 樊莉
2008-09-03
Rights Holder中国科学院新疆理化技术研究所
Date Available2013-11-27
Country中国
Subtype发明
Abstract本发明涉及一种用微波反应制备壬二酸的方法,该方法将油酸,钨酸,溶剂,搅拌混合均匀升温,滴加过氧化氢溶液,升温后,旋转蒸发回收溶剂,在蒸除溶剂的油相中加入过酸,放入微波装置中,先用小火力预热,然后在中火下反应结束后从反应液中提取产物壬二酸和副产物壬酸,产品壬二酸的产率最高可达85%(以油酸计)。本发明工艺清洁,环境友好,不污染环境,无需贵金属催化剂,不需要长时间通氧气,反应中不需要高压,实施条件简单,便于进行规模化生产。
Application Date2004-09-17
Patent NumberZL200410079993.2
Status授权
Application Number200410079993.2
Document Type专利
Identifierhttp://ir.xjipc.cas.cn/handle/365002/3119
Collection新疆维吾尔自治区精细化工工程技术研究中心
资源化学研究室
Recommended Citation
GB/T 7714
吾满江.艾力,高军军,张亚刚,等. 一种用微波反应制备壬二酸的方法. ZL200410079993.2[P]. 2008-09-03.
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