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学科主题: Chemistry ; Physics
题名: Synthesis, structure, and properties of a novel hydrated borate Rb-4[B4O5(OH)(4)](2)center dot 3H(2)O
作者: Zhao Yi; Pan Shilie; Li Feng; Wang Yongjiang; Fan Xiaoyun; Dong Xiaoyu; Jia Dianzeng; Guo Jixi; Zhou Zhongxiang
通讯作者: Pan, SL
关键词: Rb-4B4O5(OH)(4)(2)center dot 3H(2)O ; Borate ; Crystal structure ; Crystal growth
刊名: SOLID STATE SCIENCES
发表日期: 2011
DOI: 10.1016/j.solidstatesciences.2010.10.013
卷: 13, 期:1, 页:82-87
收录类别: SCI
资助者: National Natural Science Foundation of China 50802110; Chinese Academe of Sciences; Scientific Research Foundation for the Returned Overseas Chinese Scholars, State Education Ministry 20091001; Natural Science Foundation of Xinjiang Uygur Autonomous Region of China 200821159, 2009211B33; Xinjiang Uygur Autonomous Region of China 200816120
摘要: Rb-4B4O5(OH)(4)2 center dot 3H(2)O has been grown by slow evaporation method with crystal sizes up to 11 mm x 7 mm x 4 mm. Its crystal structure has been determined by single-crystal X-ray diffraction and further characterized by powder X-ray diffraction (XRD). IR, and TGA. It crystallizes in the orthorhombic space group Pbcn, with a = 16.3984(14) angstrom, b = 7.7850(7) angstrom, c = 16.0763(16) angstrom, and Z = 4. It contains isolated B4O5(OH)(4)(2-) polyanions, free water molecules and Rb cations. The Rb(1) and Rb(2) atoms are coordinated by nine and ten oxygen atoms, respectively. Connections between isolated B4O5(OH)(4)(2-) polyanions are provided by Rb polyhedra and the hydrogen-bonding to form a three-dimensional network.
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内容类型: 期刊论文
URI标识: http://ir.xjipc.cas.cn/handle/365002/2811
Appears in Collections:新疆维吾尔自治区电子信息材料与器件重点实验室_期刊论文

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作者单位: Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Xinjiang Key Lab Elect Informat Mat & Devices, Urumqi 830011, Peoples R China;Xinjiang Univ, Coll Chem & Chem Engn, Urumqi 830046, Peoples R China

Recommended Citation:
Zhao Yi,Pan Shilie,Li Feng,et al. Synthesis, structure, and properties of a novel hydrated borate Rb-4[B4O5(OH)(4)](2)center dot 3H(2)O[J]. SOLID STATE SCIENCES,2011,13(1):82-87.
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文件名: synthesis, structure, and properties of a novel hydrated borate rb 4[b4o5(oh)4]2· 3h2o.pdf
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