Synthesis, structure, and properties of Li2Pb2CuB4O10 with isolated [CuB4O10](6-) units
Li Hongyi; Pan Shilie; Wu Hongping; Smit Jared P.; Poeppelmeier Kenneth R.
2011
Source PublicationJOURNAL OF ALLOYS AND COMPOUNDS
ISSN0925-8388
Volume509Issue:7Pages:3310-3313
Abstract

The copper borate Li2Pb2CuB4O40 has been synthesized in air by the standard solid-state reaction at temperature in the range 550-650 degrees C and the structure of Li2Pb2CuB4O10 was determined by single-crystal X-ray diffraction. Li2Pb2CuB4O10 crystallizes in the monoclinic space group C2/c (no. 15) with a=16.8419(12), b=4.7895(4), c = 13.8976(10)angstrom, and beta = 125.3620(10)degrees, V=914.22(12)angstrom(3), and Z=4, as determined by single-crystal X-ray diffraction. The Li2Pb2CuB4O10 structure exhibits isolated units of stoichiometry [CuB4O10](6-) that are built from CuO4 distorted square planes and triangular BO3 groups. The IR spectroscopy and thermal analysis investigations of Li2Pb2CuB4O10 are also presented.

KeywordOxide Materials Solid State Reactions Crystal Structure X-ray Diffraction
Subject AreaChemistry ; Materials Science ; Metallurgy & Metallurgical Engineering
DOI10.1016/j.jallcom.2010.11.206
Indexed BySCI
WOS IDWOS:000287570100021
Citation statistics
Cited Times:9[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.xjipc.cas.cn/handle/365002/2796
Collection新疆维吾尔自治区电子信息材料与器件重点实验室
Corresponding AuthorPan Shilie
AffiliationChinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Xinjiang Key Lab Elect Informat Mat & Devices, Urumqi 830011, Peoples R China;Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China;Northwestern Univ, Dept Chem, Evanston, IL 60208 USA
Recommended Citation
GB/T 7714
Li Hongyi,Pan Shilie,Wu Hongping,et al. Synthesis, structure, and properties of Li2Pb2CuB4O10 with isolated [CuB4O10](6-) units[J]. JOURNAL OF ALLOYS AND COMPOUNDS,2011,509(7):3310-3313.
APA Li Hongyi,Pan Shilie,Wu Hongping,Smit Jared P.,&Poeppelmeier Kenneth R..(2011).Synthesis, structure, and properties of Li2Pb2CuB4O10 with isolated [CuB4O10](6-) units.JOURNAL OF ALLOYS AND COMPOUNDS,509(7),3310-3313.
MLA Li Hongyi,et al."Synthesis, structure, and properties of Li2Pb2CuB4O10 with isolated [CuB4O10](6-) units".JOURNAL OF ALLOYS AND COMPOUNDS 509.7(2011):3310-3313.
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