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学科主题: Chemistry
题名: Synthesis, structure and characterization of layered Ca[B(C6H6O7)(2)](H2O)(4)center dot HCl
作者: Wu Hongping; Pan Shilie; Yu Hongwei; Huang Zhenjun; Jia Dianzeng
通讯作者: Pan, SL
关键词: CaB(C6H6O7)(2)(H2O)(4)center dot HCl ; Crystal structure ; Crystal growth ; Inorganic-organic borate
刊名: JOURNAL OF MOLECULAR STRUCTURE
发表日期: 2012
DOI: 10.1016/j.molstruc.2012.05.072
卷: 1027, 期:11, 页:111-115
收录类别: SCI
资助者: Main Direction Program of Knowledge Innovation of Chinese Academy of Sciences KJCX2-EW-209-3, KJCX2-EW-H03-03; National Natural Science Foundation of China 50802110, 21001114, 21065012; "One Hundred Talents Project Foundation Program" of Chinese Academy of Sciences; "Western Light Joint Scholar Foundation" Program of Chinese Academy of Sciences; "High Technology Research and Development Program" of Xinjiang Uygur Autonomous Region of China 201116143; Natural Science Foundation of Xinjiang Uygur Autonomous Region of China 200821159, 2009211B33, 200821166; Scientific Research Program of Urumqi of China G09212001; Science and Technology in Support of Xinjiang 201091244
摘要: Introduction of the citric acid in the borate system generates a new phase. CaB(C6H6O7)(2)(H2O)(4)center dot HCl, which is transparent from 195 nm to near infrared region. Single crystals of CaB(C6H6O7)(2)(H2O)(4)center dot HCl with dimensions up to 7 x 5 x 2 mm(3) were successfully grown by slow evaporation method at room temperature. It has been characterized by single crystal X-ray diffraction, infrared spectroscopy measure and thermogravimetric analysis. CaB(C6H6O7)(2)(H2O)(4)center dot HCl crystallizes in the triclinic space group P - 1, with a = 6.3243(18) angstrom, b = 8.365(2) angstrom, c = 19.042(5) angstrom, alpha = 97.291(3)degrees, beta = 94.535(4)degrees, gamma = 94.165(4)degrees. It exhibits a unique layered structure, the layers are parallel arrangement of the (001) plane and stack along the c-axis.
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内容类型: 期刊论文
URI标识: http://ir.xjipc.cas.cn/handle/365002/2749
Appears in Collections:新疆维吾尔自治区电子信息材料与器件重点实验室_期刊论文

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作者单位: Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Xinjiang Key Lab Elect Informat Mat & Devices, Urumqi 830011, Peoples R China;Xinjiang Univ, Coll Chem & Chem Engn, Urumqi 830046, Peoples R China

Recommended Citation:
Wu Hongping,Pan Shilie,Yu Hongwei,et al. Synthesis, structure and characterization of layered Ca[B(C6H6O7)(2)](H2O)(4)center dot HCl[J]. JOURNAL OF MOLECULAR STRUCTURE,2012,1027(11):111-115.
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文件名: Synthesis, structure and characterization of layered Ca[B(C6H6O7)(2)](H2O)(4)center dot HCl.pdf
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