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学科主题: Chemistry ; Crystallography
题名: synthesis, crystal growth and characterization of a new noncentrosymmetric borophosphate: rbpbbp2o8
作者: Wang Ying; Pan Shilie; Zhang Min; Han Shujuan; Su Xin; Dong Lingyun
刊名: CRYSTENGCOMM
发表日期: 2013
DOI: 10.1039/c3ce40394g
卷: 15, 期:24, 页:4956-4962
收录类别: SCI
资助者: Western Light of Chinese Academy of Sciences XBBS201220, XBBS201217; 973 Program of China 2012CB626803; National Natural Science Foundation of China U1129301, 51172277, 21101168, 11104344; Main Direction Program of Knowledge Innovation of CAS KJCX2-EW-H03-03; One Hundred Talents Project Foundation Program of CAS; Funds for Creative Cross & Cooperation Teams of CAS; Major Program of Xinjiang Uygur Autonomous Region of China during the 12th Five-Year Plan Period 201130111; High Technology Research & Development Program of Xinjiang Uygur Autonomous Region of China 201116143; Science and Technology Project of Urumqi G121130002
摘要: A new noncentrosymmetric borophosphate, RbPbBP2O8, has been synthesized and its high quality single crystal with dimensions up to 23 mm x 18 mm x 7 mm was successfully grown by the Kyropoulos method for the first time. It crystallizes in the tetragonal system, space group I42d with cell parameters a = 7.213(3) angstrom, c = 13.987(10) angstrom, Z = 4, V = 727.8(6) angstrom(3). The structure analysis reveals that RbPbBP2O8 features a three-dimensional framework composed of BO4 and PO4 tetrahedra interconnected by MO8 (M = Rb/Pb) distorted polyhedra. The powder second harmonic generation effect of RbPbBP2O8 is similar to that of KH2PO4. Thermal analysis and transmittance spectroscopy were also performed on the reported crystal.
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内容类型: 期刊论文
URI标识: http://ir.xjipc.cas.cn/handle/365002/2698
Appears in Collections:新疆维吾尔自治区电子信息材料与器件重点实验室_期刊论文

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作者单位: Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Key Lab Funct Mat & Devices Special Environm, Urumqi 830011, Peoples R China;Univ Chinese Acad Sci, Beijing 100049, Peoples R China

Recommended Citation:
Wang Ying,Pan Shilie,Zhang Min,et al. synthesis, crystal growth and characterization of a new noncentrosymmetric borophosphate: rbpbbp2o8[J]. CRYSTENGCOMM,2013,15(24):4956-4962.
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文件名: synthesis, crystal growth and characterization of a new noncentrosymmetric borophosphate rbpbbp2o8.pdf
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