SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY
Yang Yi; Bakri Mahinur; Gu Dongyu; Aisa Haji Akber; Aisa, HA
2013
发表期刊JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES
ISSN1082-6076
卷号36期号:5页码:573-582
摘要

An effective high-speed countercurrent chromatography (HSCCC) method was established for separation and purification of (S)-dehydrovomifoliol from the leaves of Nitraria sibirica Pall. (NS). HSCCC was performed with a two-phase solvent systems composed of n-hexane-ethyl acetate-methanol-water (1:5:1:5, v/v) at a flow rate of 2mL/min. From 1g crude sample of NS, 23mg (S)-dehydrovomifoliol was obtained at purity of 95%. The chemical structure was confirmed by MS, 1H NMR, and 13C NMR. (S)-dehydrovomifoliol was isolated from Nitraria genus for the first time.

关键词Bioactive Compound (s)-dehydrovomifoliol High-speed Counter-current Chromatography Nitraria Sibirica Pall Separation Traditional Uighur Medicine
学科领域Biochemistry & Molecular Biology ; Chemistry
DOI10.1080/10826076.2012.668738
收录类别SCI
WOS记录号WOS:000315349900003
引用统计
被引频次:7[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.xjipc.cas.cn/handle/365002/2685
专题省部共建新疆特有药用资源利用重点实验室
通讯作者Aisa, HA
作者单位Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Key Lab Xinjiang Indigenous Med Plants Resource U, Urumqi 830011, Peoples R China;Chinese Acad Sci, Grad Univ, Beijing, Peoples R China
推荐引用方式
GB/T 7714
Yang Yi,Bakri Mahinur,Gu Dongyu,et al. SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY[J]. JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,2013,36(5):573-582.
APA Yang Yi,Bakri Mahinur,Gu Dongyu,Aisa Haji Akber,&Aisa, HA.(2013).SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY.JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,36(5),573-582.
MLA Yang Yi,et al."SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY".JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES 36.5(2013):573-582.
条目包含的文件
文件名称/大小 文献类型 版本类型 开放类型 使用许可
SEPARATION OF (S)-DE(511KB)期刊论文作者接受稿开放获取CC BY-NC-SA浏览 请求全文
个性服务
推荐该条目
保存到收藏夹
查看访问统计
导出为Endnote文件
谷歌学术
谷歌学术中相似的文章
[Yang Yi]的文章
[Bakri Mahinur]的文章
[Gu Dongyu]的文章
百度学术
百度学术中相似的文章
[Yang Yi]的文章
[Bakri Mahinur]的文章
[Gu Dongyu]的文章
必应学术
必应学术中相似的文章
[Yang Yi]的文章
[Bakri Mahinur]的文章
[Gu Dongyu]的文章
相关权益政策
暂无数据
收藏/分享
文件名: SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY.pdf
格式: Adobe PDF
所有评论 (0)
暂无评论
 

除非特别说明,本系统中所有内容都受版权保护,并保留所有权利。