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学科主题: Biochemistry & Molecular Biology ; Chemistry
题名: SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY
作者: Yang Yi; Bakri Mahinur; Gu Dongyu; Aisa Haji Akber
通讯作者: Aisa, HA
关键词: bioactive compound ; (S)-dehydrovomifoliol ; high-speed counter-current chromatography ; Nitraria sibirica Pall ; separation ; traditional Uighur Medicine
刊名: JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES
发表日期: 2013
DOI: 10.1080/10826076.2012.668738
卷: 36, 期:5, 页:573-582
收录类别: SCI
资助者: West Light Foundation of The Chinese Academy of Sciences XBBS201011; China National Funds for Distinguished Young Scientists 30925045
摘要: An effective high-speed countercurrent chromatography (HSCCC) method was established for separation and purification of (S)-dehydrovomifoliol from the leaves of Nitraria sibirica Pall. (NS). HSCCC was performed with a two-phase solvent systems composed of n-hexane-ethyl acetate-methanol-water (1:5:1:5, v/v) at a flow rate of 2mL/min. From 1g crude sample of NS, 23mg (S)-dehydrovomifoliol was obtained at purity of 95%. The chemical structure was confirmed by MS, 1H NMR, and 13C NMR. (S)-dehydrovomifoliol was isolated from Nitraria genus for the first time.
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内容类型: 期刊论文
URI标识: http://ir.xjipc.cas.cn/handle/365002/2685
Appears in Collections:新疆维吾尔自治区植物资源化学重点实验室 _期刊论文

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SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY.pdf(511KB)期刊论文作者接受稿开放获取View 联系获取全文

作者单位: Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Key Lab Xinjiang Indigenous Med Plants Resource U, Urumqi 830011, Peoples R China;Chinese Acad Sci, Grad Univ, Beijing, Peoples R China

Recommended Citation:
Yang Yi,Bakri Mahinur,Gu Dongyu,et al. SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY[J]. JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,2013,36(5):573-582.
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文件名: SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY.pdf
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