XJIPC OpenIR  > 省部共建新疆特有药用资源利用重点实验室
SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY
Yang Yi; Bakri Mahinur; Gu Dongyu; Aisa Haji Akber
2013
Source PublicationJOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES
ISSN1082-6076
Volume36Issue:5Pages:573-582
Abstract

An effective high-speed countercurrent chromatography (HSCCC) method was established for separation and purification of (S)-dehydrovomifoliol from the leaves of Nitraria sibirica Pall. (NS). HSCCC was performed with a two-phase solvent systems composed of n-hexane-ethyl acetate-methanol-water (1:5:1:5, v/v) at a flow rate of 2mL/min. From 1g crude sample of NS, 23mg (S)-dehydrovomifoliol was obtained at purity of 95%. The chemical structure was confirmed by MS, 1H NMR, and 13C NMR. (S)-dehydrovomifoliol was isolated from Nitraria genus for the first time.

KeywordBioactive Compound (s)-dehydrovomifoliol High-speed Counter-current Chromatography Nitraria Sibirica Pall Separation Traditional Uighur Medicine
Subject AreaBiochemistry & Molecular Biology ; Chemistry
DOI10.1080/10826076.2012.668738
Indexed BySCI
WOS IDWOS:000315349900003
Citation statistics
Document Type期刊论文
Identifierhttp://ir.xjipc.cas.cn/handle/365002/2685
Collection省部共建新疆特有药用资源利用重点实验室
资源化学研究室
Corresponding AuthorAisa Haji Akber
AffiliationChinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Key Lab Xinjiang Indigenous Med Plants Resource U, Urumqi 830011, Peoples R China;Chinese Acad Sci, Grad Univ, Beijing, Peoples R China
Recommended Citation
GB/T 7714
Yang Yi,Bakri Mahinur,Gu Dongyu,et al. SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY[J]. JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,2013,36(5):573-582.
APA Yang Yi,Bakri Mahinur,Gu Dongyu,&Aisa Haji Akber.(2013).SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY.JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,36(5),573-582.
MLA Yang Yi,et al."SEPARATION OF (S)-DEHYDROVOMIFOLIOL FROM LEAVES OF NITRARIA SIBIRICA PALL. BY HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY".JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES 36.5(2013):573-582.
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