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Application of preparative high-speed countercurrent chromatography for separation of elatine from Delphinium shawurense
Yang Yi; Gu Dongyu; Wu Hankui; Aisa Haji Akber; Zhang Tianyou; Ito Yoichiro; Aisa, HA
2008
发表期刊JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES
ISSN10826076
卷号31期号:19页码:3012-3019
摘要Preparative separation of elatine in Delphinium shawurense was achieved for the first time using high speed countercurrent chromatography (HSCCC). The separation was performed with a solvent system composed of ethyl acetate-chloroform-methanol-water (3:0.1:2:3, v/v) using the lower organic phase as a mobile phase under a revolution speed of 800 rpm. This yielded 72 mg of elatine at over 97% purity with an approximately 95% recovery. The chemical structure was identified by MS and NMR.
关键词Delphinium Shawurense Elatine High Speed Countercurrent Chromatography (Hsccc)
DOI10.1080/10826070802424956
收录类别EI
WOS记录号WOS:000259695300009
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文献类型期刊论文
条目标识符http://ir.xjipc.cas.cn/handle/365002/2079
专题资源化学研究室
通讯作者Aisa, HA
作者单位Chinese Acad Sci, Xinjiang Key Lab Plant Resources & Nat Prod Chem, Xinjiang Tech Inst Phys & Chem, Urumqi, Peoples R China;Chinese Acad Sci, Grad Univ, Beijing, Peoples R China;Beijing Inst New Technol, Beijing, Peoples R China; NHLBI, Ctr Biochem & Biophys, NIH, Bethesda, MD 20892 USA
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Yang Yi,Gu Dongyu,Wu Hankui,et al. Application of preparative high-speed countercurrent chromatography for separation of elatine from Delphinium shawurense[J]. JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,2008,31(19):3012-3019.
APA Yang Yi.,Gu Dongyu.,Wu Hankui.,Aisa Haji Akber.,Zhang Tianyou.,...&Aisa, HA.(2008).Application of preparative high-speed countercurrent chromatography for separation of elatine from Delphinium shawurense.JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,31(19),3012-3019.
MLA Yang Yi,et al."Application of preparative high-speed countercurrent chromatography for separation of elatine from Delphinium shawurense".JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES 31.19(2008):3012-3019.
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