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Application of preparative high-speed countercurrent chromatography for separation of elatine from Delphinium shawurense
Yang Yi; Gu Dongyu; Wu Hankui; Aisa Haji Akber; Zhang Tianyou; Ito Yoichiro
2008
Source PublicationJOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES
ISSN1082-6076
Volume31Issue:19Pages:3012-3019
Abstract

Preparative separation of elatine in Delphinium shawurense was achieved for the first time using high speed countercurrent chromatography (HSCCC). The separation was performed with a solvent system composed of ethyl acetate-chloroform-methanol-water (3:0.1:2:3, v/v) using the lower organic phase as a mobile phase under a revolution speed of 800 rpm. This yielded 72 mg of elatine at over 97% purity with an approximately 95% recovery. The chemical structure was identified by MS and NMR.

KeywordDelphinium Shawurense Elatine High Speed Countercurrent Chromatography (Hsccc)
DOI10.1080/10826070802424956
Indexed BySCI
WOS IDWOS:000259695300009
Citation statistics
Cited Times:25[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.xjipc.cas.cn/handle/365002/2079
Collection资源化学研究室
Corresponding AuthorAisa Haji Akber
Affiliation1.Chinese Acad Sci, Xinjiang Key Lab Plant Resources & Nat Prod Chem, Xinjiang Tech Inst Phys & Chem, Urumqi, Peoples R China
2.Chinese Acad Sci, Grad Univ, Beijing, Peoples R China
3.Beijing Inst New Technol, Beijing, Peoples R China
Recommended Citation
GB/T 7714
Yang Yi,Gu Dongyu,Wu Hankui,et al. Application of preparative high-speed countercurrent chromatography for separation of elatine from Delphinium shawurense[J]. JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,2008,31(19):3012-3019.
APA Yang Yi,Gu Dongyu,Wu Hankui,Aisa Haji Akber,Zhang Tianyou,&Ito Yoichiro.(2008).Application of preparative high-speed countercurrent chromatography for separation of elatine from Delphinium shawurense.JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,31(19),3012-3019.
MLA Yang Yi,et al."Application of preparative high-speed countercurrent chromatography for separation of elatine from Delphinium shawurense".JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES 31.19(2008):3012-3019.
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