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Preparation and characterization of Mn0.43Ni0.9CuFe0.67O4 by a polymerized complex method
Wang Shao-Gang; Chang Ai-Min; Zhang Hui-Min; Zhao Qing
2008
Source PublicationMaterials Chemistry and Physics
ISSN2540584
Volume110Issue:1Pages:83-88
AbstractMn0.43Ni0.9CuFe0.67O4 nano-sized powders were synthesized by the Pechini method for the first time. A spinel-type phase was attained from calcining of the polymerized gel precursor at 400-700 °C. The thermal evolution, surface morphology, and structural behavior have been studied by TG/DTA, SEM, XRD and FT-IR. It was found that the material decomposes upon heating above 300 °C. The monoclinic structure of CuO was found to be coexistent with the spinel-type phase in both the calcined powders and the sintered ceramics. The electrical properties were deeply affected by the crystal phase of CuO. The ceramics sintered at 1100 °C showed the best electrical properties as well as the density, of which the relative density was measured to be about 96%. The resistivity ρ25 °C is about 600 Ω cm and B25 °C/50 °C is about 2000.
KeywordCeramics Microstructure Sintering Electrical Properties
DOI10.1016/j.matchemphys.2008.01.019
Indexed BySCI
WOS IDWOS:000256114400015
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Cited Times:15[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.xjipc.cas.cn/handle/365002/1986
Collection材料物理与化学研究室
AffiliationChinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Urumqi 830011, Peoples R China;Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China
Recommended Citation
GB/T 7714
Wang Shao-Gang,Chang Ai-Min,Zhang Hui-Min,et al. Preparation and characterization of Mn0.43Ni0.9CuFe0.67O4 by a polymerized complex method[J]. Materials Chemistry and Physics,2008,110(1):83-88.
APA Wang Shao-Gang,Chang Ai-Min,Zhang Hui-Min,&Zhao Qing.(2008).Preparation and characterization of Mn0.43Ni0.9CuFe0.67O4 by a polymerized complex method.Materials Chemistry and Physics,110(1),83-88.
MLA Wang Shao-Gang,et al."Preparation and characterization of Mn0.43Ni0.9CuFe0.67O4 by a polymerized complex method".Materials Chemistry and Physics 110.1(2008):83-88.
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