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高效液相色谱法测定芹菜籽中3-正丁基苯酞的含量
Alternative Titledetermination of 3 -n -butylphthalide in celery seed by hplc
顾冬雨; 吕金良; 古丽娜·沙比尔; 阿吉艾克拜尔·艾萨
2007
Source Publication时珍国医国药
ISSN1008-0805
Volume18Issue:3Pages:513-514
Abstract目的高效液相色谱(HPLC)法测定芹菜籽中3-正丁基苯酞的含量。方法采用YMC ODS C18柱(250 mm×4.6mm,5μm);流动相为乙腈-酯酸钠(45∶55),酯酸钠0.05 mol.L-1,冰酯酸调节pH4.6;检测波长为228 nm;流速为1.0ml.min-1;柱温:40℃。结果3-正丁基苯酞在0.044 1~0.161 7μg范围内线性关系良好,r=0.999 7,方法的回收率为98.19%,RSD为1.38%(n=5)。结论该方法能够准确可靠地测定3-正丁基苯酞的含量,可作为芹菜籽的质量控制指标之一。
Keyword芹菜籽 3-正丁基苯酞 高效液相色谱法
Document Type期刊论文
Identifierhttp://ir.xjipc.cas.cn/handle/365002/1980
Collection省部共建新疆特有药用资源利用重点实验室
资源化学研究室
Affiliation中国科学院新疆理化技术研究所新疆植物资源化学重点实验室;新疆中药民族药研究所;中国科学院研究生院
Recommended Citation
GB/T 7714
顾冬雨,吕金良,古丽娜·沙比尔,等. 高效液相色谱法测定芹菜籽中3-正丁基苯酞的含量[J]. 时珍国医国药,2007,18(3):513-514.
APA 顾冬雨,吕金良,古丽娜·沙比尔,&阿吉艾克拜尔·艾萨.(2007).高效液相色谱法测定芹菜籽中3-正丁基苯酞的含量.时珍国医国药,18(3),513-514.
MLA 顾冬雨,et al."高效液相色谱法测定芹菜籽中3-正丁基苯酞的含量".时珍国医国药 18.3(2007):513-514.
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