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Preparative isolation and purification of four flavonoids from Flos Gossypii by high-speed countercurrent chromatography
Yang Yi; Wu Tao; Yang Wu Xing; Aisa Haji Akber; Zhang Tian You; Ito Yoichiro
2008
发表期刊JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES
ISSN10826076
卷号31期号:10页码:1523-1531
摘要Following an initial cleanup step on the AB-8 macroporous resin, high-speed countercurrent chromatography (HSCCC) was successfully applied for the first time to the isolation and purification of four flavonoids from Flos Gossypii. HSCCC was performed with a two-phase solvent system composed of chloroform-methanol-isopropanol-water (5:5:1:3, v/v) adding 0.4% phosphoric acid in the aqueous stationary phase. The separation yielded quercetin (5.6 mg), quercetin-3′-O-D-glucoside (7.2 mg), quercetin-3-O-β-D-glucoside (16 mg), quercetin-7-O-β-D-glucoside (8.3 mg), from 100 mg of the crude extract in a one step separation. The structure identification was made by 1H NMR, 13C NMR.
关键词High-speed Countercurrent Chromatography Flos Gossypii Flavonoids
DOI10.1080/10826070802039663
收录类别EI
WOS记录号WOS:000255272900011
引用统计
被引频次:13[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.xjipc.cas.cn/handle/365002/1927
专题资源化学研究室
作者单位NHLBI, Biochem & Biophys Ctr, NIH, Bethesda, MD 20892 USA;Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Xinjiang Key Lab Plant Resources & Nat Prod Chem, Urumqi, Peoples R China;Chinese Acad Sci, Grad Univ, Beijing, Peoples R China;Beijing Inst New Technol Applicat, Beijing, Peoples R China
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Yang Yi,Wu Tao,Yang Wu Xing,et al. Preparative isolation and purification of four flavonoids from Flos Gossypii by high-speed countercurrent chromatography[J]. JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,2008,31(10):1523-1531.
APA Yang Yi,Wu Tao,Yang Wu Xing,Aisa Haji Akber,Zhang Tian You,&Ito Yoichiro.(2008).Preparative isolation and purification of four flavonoids from Flos Gossypii by high-speed countercurrent chromatography.JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,31(10),1523-1531.
MLA Yang Yi,et al."Preparative isolation and purification of four flavonoids from Flos Gossypii by high-speed countercurrent chromatography".JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES 31.10(2008):1523-1531.
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