NOVEL DESIGN FOR CENTRIFUGAL COUNTERCURRENT CHROMATOGRAPHY: II. STUDIES ON NOVEL GEOMETRIES OF ZIGZAG TOROIDAL TUBING
Yang Yi; Aisa Haji Akber; Ito Yoichiro
2010
发表期刊JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES
ISSN10826076
卷号33期号:3页码:336-348
摘要The toroidal column using a zigzag pattern has been improved in both retention of the stationary phase and peak resolution. To further improve the retention of stationary phase and peak resolution, a series of novel geometric designs of tubing (plain, mid clamping, flattened, and flat twisted tubing) was evaluated for their performance in CCC. The results showed that the tubing, which was flattened vertically against the centrifugal force (vert-flattened tubing) produced the best peak resolution among them. Using vert-flattened tubing a series of experiments was performed to study the effects of column capacity and sample size. The results indicated that a 0.25mL capacity column is ideal for analysis of small amount samples.
关键词Clamped Tubing Countercurrent Chromatography Flattened Tubing Flat Twisted Tubing Resolution Zigzag Toroidal Column
学科领域Biochemistry & Molecular Biology ; Chemistry
DOI10.1080/10826070903524100
WOS记录号WOS:000274174400004
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被引频次:12[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.xjipc.cas.cn/handle/365002/1846
专题省部共建新疆特有药用资源利用重点实验室
作者单位NHLBI, Bioseparat Technol Lab, Biochem & Biophys Ctr, NIH, Bethesda, MD 20892 USA;Chinese Acad Sci, Xinjiang Key Lab Plant Resources & Nat Prod Chem, Xinjiang Tech Inst Phys & Chem, Urumqi, Peoples R China;Chinese Acad Sci, Grad Univ, Beijing, Peoples R China
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Yang Yi,Aisa Haji Akber,Ito Yoichiro. NOVEL DESIGN FOR CENTRIFUGAL COUNTERCURRENT CHROMATOGRAPHY: II. STUDIES ON NOVEL GEOMETRIES OF ZIGZAG TOROIDAL TUBING[J]. JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,2010,33(3):336-348.
APA Yang Yi,Aisa Haji Akber,&Ito Yoichiro.(2010).NOVEL DESIGN FOR CENTRIFUGAL COUNTERCURRENT CHROMATOGRAPHY: II. STUDIES ON NOVEL GEOMETRIES OF ZIGZAG TOROIDAL TUBING.JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,33(3),336-348.
MLA Yang Yi,et al."NOVEL DESIGN FOR CENTRIFUGAL COUNTERCURRENT CHROMATOGRAPHY: II. STUDIES ON NOVEL GEOMETRIES OF ZIGZAG TOROIDAL TUBING".JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES 33.3(2010):336-348.
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