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玫瑰花药材的HPLC指纹图谱研究
Alternative Titlefingerprints of rosae rugosae flos by hplc
马依努尔·拜克力; 陈君; 仲婕; 阿吉艾克拜尔·艾萨
2011
Source Publication中药材
ISSN1001-4454
Volume34Issue:7Pages:1043-1046
Abstract

目的:采用HPLC法建立新疆和田玫瑰花药材的指纹图谱。方法:色谱柱Inertsil ODS-3(4.6 mm×250mm,5μm),流动相为A[甲醇∶乙腈(1∶1)]-B(0.06%的三氟乙酸溶液),程序梯度洗脱;流速:1.0 mL/min;柱温:32℃;检测波长:254 nm。结果:检测了13批玫瑰花药材,标定了9个共有峰,相似度较好,达到了中药指纹图谱研究的技术要求。结论:本方法准确、可靠,建立的HPLC指纹图谱为玫瑰花药材的质量控制提供更全面的信息。

Other Abstract

bjective:To establish a HPLC fingerprint of Rosae Rugosae Flos.Methods:Inertsil ODS-3(4.6 mm * 250 mm,5 mum)was used with the mixture of methanol,acetonitrile and 0.06% TFA as mobile phase.The flow rate was 1.0 mL / min,the column temperature was 32℃ ,and the detection wavelength was 254 nm.Results:HPLC fingerprint of 9 main peaks was established preliminarily from 13 samples of Rosae Rugosae Flos which achieved the technical requirements of the fingerprint of traditional Chinese medicine.Conclusion:The method is reliable,accurate and can be used for quality comtrol of Rosae Rugosae Flos.

Keyword玫瑰花 Hplc 指纹图谱
Subject AreaGeneral & Internal Medicine (Provided By Thomson Reuters)
Indexed ByCSCD
CSCD IDCSCD:4329819
Citation statistics
Cited Times:2[CSCD]   [CSCD Record]
Document Type期刊论文
Identifierhttp://ir.xjipc.cas.cn/handle/365002/1593
Collection省部共建新疆特有药用资源利用重点实验室
资源化学研究室
Corresponding Author阿吉艾克拜尔·艾萨
Affiliation中国科学院新疆理化技术研究所植物资源化学重点实验室
Recommended Citation
GB/T 7714
马依努尔·拜克力,陈君,仲婕,等. 玫瑰花药材的HPLC指纹图谱研究[J]. 中药材,2011,34(7):1043-1046.
APA 马依努尔·拜克力,陈君,仲婕,&阿吉艾克拜尔·艾萨.(2011).玫瑰花药材的HPLC指纹图谱研究.中药材,34(7),1043-1046.
MLA 马依努尔·拜克力,et al."玫瑰花药材的HPLC指纹图谱研究".中药材 34.7(2011):1043-1046.
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