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己二酮糖硝基甲烷加合产物的结构确定
Alternative Titlecharacterizing the adduct of diketohexose with nitromethane by nmr spectroscopy
贺耀武; 孙万赋; 曹玲华; 周树宝; 阿吉艾克拜尔·艾萨
2011
Source Publication波谱学杂志
ISSN1000-4556
Volume28Issue:2Pages:272-277
Abstract

立体选择性地合成了1,2:4,5-二-O-异亚丙基-3-C-硝基甲基-β-D-核-己-2-吡喃酮糖,确证了其绝对构型.并用gCOSY、gHSQC、gHMBC、ROESY等2D NMR技术对它的1H和13C NMR谱峰进行了全归属.

Other Abstract

1,2 :4,5-di-0-isopropylidene-3-C-nitromethyl-beta-D-ribo-hex-2-ulo pyranose was synthesized with high stereoselectivity.Its absolute configuration was confirmed.The ~1H and ~(13)C NMR signals of the compound were assigned using ID and 2D techniques,including H NMR,~(13)C NMR,gCOSY,gHSQC,gHMBC and ROESY.

Keyword核磁共振(Nmr) 归属 己二酮糖 加合物
Subject AreaChemistry (Provided By Thomson Reuters)
Indexed ByCSCD
CSCD IDCSCD:4212965
Citation statistics
Cited Times:1[CSCD]   [CSCD Record]
Document Type期刊论文
Identifierhttp://ir.xjipc.cas.cn/handle/365002/1550
Collection资源化学研究室
Corresponding Author阿吉艾克拜尔·艾萨
Affiliation中国科学院干旱区植物资源化学重点实验室中国科学院新疆理化技术研究所;中国科学院研究生院;新疆大学理化测试中心;新疆大学化学化工学院
Recommended Citation
GB/T 7714
贺耀武,孙万赋,曹玲华,等. 己二酮糖硝基甲烷加合产物的结构确定[J]. 波谱学杂志,2011,28(2):272-277.
APA 贺耀武,孙万赋,曹玲华,周树宝,&阿吉艾克拜尔·艾萨.(2011).己二酮糖硝基甲烷加合产物的结构确定.波谱学杂志,28(2),272-277.
MLA 贺耀武,et al."己二酮糖硝基甲烷加合产物的结构确定".波谱学杂志 28.2(2011):272-277.
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