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甘草次酸/11-脱氧甘草次酸甲酯的合成
Alternative Titlesynthesis of glycyrrhetinic acid, 11 - deoxylglycyrrhetinic acid methyl ester
雍建平; 阿吉艾克拜尔·艾萨
2011
Source Publication时珍国医国药
ISSN1008-0805
Volume22Issue:11Pages:2618-2619
Abstract以甘草次酸为原料,采用经典的克莱门森还原制备了11-脱氧甘草次酸,接着在不同的催化体系中(浓硫酸、浓盐酸、干盐酸气)研究了合成了甘草次酸甲酯的最佳条件,结果表明以干盐酸气催化可获得较高的产率。并在该条件下合成了11-脱氧甘草次酸甲酯。合成的化合物经过IR,1HNMR,13CNMR等进行了表征。
Other Abstract11-deoxylglycyrrhetinic acid was synthesized by Clemmensen reduction using glycyrrhetinic acid as starting material. Then, their methyl esters were also synthesized catalyzed by different catalyst (dry HCl gas, concentrated H2SO4, concentrated HCl). The results showed that it will obtain the good yield catalyzed by dry HCl gas among the above catalysts. The synthesized compounds were confirmed by IR, 1HNMR, 13CNMR and MS.
Keyword甘草次酸 11-脱氧甘草次酸 克莱门森还原 酯化反应
Subject AreaGeneral & Internal Medicine (Provided By Thomson Reuters)
Indexed ByCSCD
CSCD IDCSCD:4375719
Citation statistics
Cited Times:2[CSCD]   [CSCD Record]
Document Type期刊论文
Identifierhttp://ir.xjipc.cas.cn/handle/365002/1471
Collection资源化学研究室
Affiliation宁夏医科大学公卫学院;中国科学院新疆理化技术研究所
Recommended Citation
GB/T 7714
雍建平,阿吉艾克拜尔·艾萨. 甘草次酸/11-脱氧甘草次酸甲酯的合成[J]. 时珍国医国药,2011,22(11):2618-2619.
APA 雍建平,&阿吉艾克拜尔·艾萨.(2011).甘草次酸/11-脱氧甘草次酸甲酯的合成.时珍国医国药,22(11),2618-2619.
MLA 雍建平,et al."甘草次酸/11-脱氧甘草次酸甲酯的合成".时珍国医国药 22.11(2011):2618-2619.
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