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学科主题: Materials Science
题名:
Synthesis, structure, and properties of the non-centrosymmetric borate Rb2CaB8O26H24
作者: Luo Jiang; Pan ShiLie(潘世烈); Li Hongyi; Zhou Zhongxiang; Yang Zhihua
通讯作者: Pan, SL
刊名: Journal of Materials Science
发表日期: 2011
DOI: 10.1007/s10853-011-5710-6
卷: 46, 期:23, 页:7443-7448
收录类别: SCI
摘要: Single crystals of Rb2CaB8O26H24, a new noncentrosymmetric borate material, have been grown with sizes up to 8 9 5 9 3 mm3 by the slow evaporation of water solution at room temperature. The structure of the compound was determined by single-crystal X-ray diffraction. It crystallizes in the orthorhombic system, space group P212121 with a = 11.5288(3) A ° , b = 12.6 334(4) A ° , c = 16.6966(4) A ° , Z = 4 and R1 = 0.0405, wR2 = 0.1043. Ultraviolet (UV)-vis spectrum transmission is performed on the Rb2CaB8O26H24, which shows an absorption edge about 195 nm in the UV region. Thermal properties were investigated by TG-DSC analysis. The powder second-harmonic generation (SHG) intensity measured by the Kurtz-Perry method indicates that Rb2CaB8O26H24 has about one-third of KDP (KH2PO4). The influence of different molar ratios and evaporation speed of water solution on crystal quality and size was also performed on the reported material.
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内容类型: 期刊论文
URI标识: http://ir.xjipc.cas.cn/handle/365002/1439
Appears in Collections:新疆维吾尔自治区电子信息材料与器件重点实验室_期刊论文

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作者单位: Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Xinjiang Key Lab Elect Informat Mat & Devices, Urumqi 830011, Peoples R China;Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China

Recommended Citation:
Luo Jiang,Pan Shilie,Li Hongyi,et al. Synthesis, structure, and properties of the non-centrosymmetric borate Rb2CaB8O26H24[J]. Journal of Materials Science,2011-01-01,46(23):7443-7448.
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文件名: synthesis, structure, and properties of the non-centrosymmetric borate rb2cab8o26h24.pdf
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