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学科主题: Chemistry
题名: Li2Sr4B12O23: A new alkali and alkaline-earth metal mixed borate with [B10O18](6-) network and isolated [B2O5](4-) unit
作者: Zhang Min; Pan Shilie; Han Jian; Yang Zhihua; Su Xin; Zhao Wenwu
通讯作者: Pan, SL
关键词: Li2Sr4B12O23 ; Crystal structure ; Crystal growth ; Borate
刊名: Journal of Solid State Chemistry
发表日期: 2012
DOI: 10.1016/j.jssc.2012.01.061
卷: 190, 期:6, 页:92-97
收录类别: SCI
资助者: Natural Science Foundation of Xinjiang Uygur Autonomous Region of China 200821159, 2009211833; Chinese Academy of Sciences KJCX2-EW-209-3, KJCX2-EW-H03-03; National Natural Science Foundation of China 50802110, 21001114; "Western Light Joint Scholar Foundation" of Chinese Academy of Sciences; Xinjiang Uygur Autonomous Region of China 201116143
摘要: A novel ternary lithium strontium borate Li2Sr4B 12O23 crystal with size up to 20 mm×10 mm×4 mm has been grown via the top-seeded solution growth method below 730 °C. Single-crystal XRD analyses showed that Li2Sr4B 12O23 crystallizes in the monoclinic space group P2 1/c with a=6.4664(4) A˚, b=8.4878(4) A˚, c=15.3337(8) A˚, β=102.02(3)°, Z=2. The crystal structure is composed of [B10O18]6- network and isolated [B 2O5]4- unit. The IR spectrum further confirmed the presence of both BO3 and BO4 groups. TG-DSC and Transmission spectrum were reported. Band structures and density of states were calculated.
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内容类型: 期刊论文
URI标识: http://ir.xjipc.cas.cn/handle/365002/1402
Appears in Collections:新疆维吾尔自治区电子信息材料与器件重点实验室_期刊论文

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作者单位: Chinese Acad Sci, Xinjiang Key Lab Elect Informat Mat & Devices, Xinjiang Tech Inst Phys & Chem, Urumqi 830011, Peoples R China;Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China

Recommended Citation:
Zhang Min,Pan Shilie,Han Jian,et al. Li2Sr4B12O23: A new alkali and alkaline-earth metal mixed borate with [B10O18](6-) network and isolated [B2O5](4-) unit[J]. Journal of Solid State Chemistry,2012,190(6):92-97.
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