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学科主题: Chemistry ; Physics
题名: synthesis, crystal structure and properties of a new congruently melting compound, k3znb5o10
作者: Wu Hongping; Pan Shilie; Yu Hongwei; Chen Zhaohui; Zhang Fangfang
通讯作者: Pan, SL
关键词: K3ZnB5O10 ; Single crystal growth ; X-ray diffraction ; Optical properties
刊名: Solid State Sciences
发表日期: 2012
DOI: 10.1016/j.solidstatesciences.2012.04.035
卷: 14, 期:7, 页:936-940
收录类别: SCI
摘要: A new compound, K3ZnB5O10, has been synthesized by solid-state reaction. It crystallizes in the monoclinic system, space group P21/n with unit-cell parameters a = 7.6391(5) A˚, b = 19.2304(13) A˚, c = 7.6905(5) A˚, β = 116.698(4)° and Z = 4. The structure of the compound is solved by the direct methods and refined to R1 = 0.0286 and wR2 = 0.0600. K3ZnB5O10 contains a two-dimensional ZnB5O10 layer, which forms by connecting isolated double ring [B5O10] groups and ZnO4 tetrahedra. The K atoms filling in the interlayer and intralayer link the layers together. Functional groups presented in the sample were identified by FTIR spectrum. UV-vis-NIR diffuse reflectance spectrum exhibits ultraviolet cutoff edge is about 190 nm. The DSC analysis proves that K 3ZnB5O10 is a congruently melting compound.
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内容类型: 期刊论文
URI标识: http://ir.xjipc.cas.cn/handle/365002/1382
Appears in Collections:新疆维吾尔自治区电子信息材料与器件重点实验室_期刊论文

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作者单位: Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Xinjiang Key Lab Elect Informat Mat & Devices, Urumqi 830011, Peoples R China; Xinjiang Univ, Coll Chem & Chem Engn, Urumqi 830046, Peoples R China

Recommended Citation:
Wu Hongping,Pan Shilie,Yu Hongwei,et al. synthesis, crystal structure and properties of a new congruently melting compound, k3znb5o10[J]. Solid State Sciences,2012,14(7):936-940.
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文件名: synthesis, crystal structure and properties of a new congruently melting compound, k3znb5o10.pdf
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