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学科主题: Materials Science
题名: Synthesis, crystal structure and properties of a new lead fluoride borate, Pb3OBO3F
作者: Zhao Wenwu; Pan Shilie; Dong Xiaoyu; Li Junjie; Tian Xuelin; Fan Xiaoyun; Chen Zhaohui; Zhang Fangfang
通讯作者: Pan, SL
关键词: X-ray diffraction ; Crystal structure ; Optical properties
刊名: Materials Research Bulletin
发表日期: 2012
DOI: 10.1016/j.materresbull.2012.01.019
卷: 47, 期:4, 页:947-951
收录类别: SCI
摘要: A new compound, Pb3OBO3F, has been grown by the high temperature solution method from the PbO-PbF2-B2O 3 system. It crystallizes in the orthorhombic system, space group Pbcm with unit-cell parameters a = 7.6313(14) , b = 6.5229(12) , c = 11.906(2) , Z = 4, volume = 592.66(19) 3. The structure of the compound is solved by the direct methods and refined to R1 = 0.0528 and wR 2 = 0.1400. Pb3OBO3F consists of Pb(1)O 3F tetrahedra, Pb(2)O4 tetrahedra and BO3 triangles which build up the symmetrical chains extended along the c-axis. The powder X-ray diffraction pattern of the Pb3OBO3F has been measured. Functional groups presented in the sample were identified by Fourier transform infrared spectrum.
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内容类型: 期刊论文
URI标识: http://ir.xjipc.cas.cn/handle/365002/1368
Appears in Collections:新疆维吾尔自治区电子信息材料与器件重点实验室_期刊论文

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作者单位: Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Xinjiang Key Lab Elect Informat Mat & Devices, Urumqi 830011, Peoples R China;Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China;Xinjiang Univ, Phys & Chem Detecting Ctr, Urumqi 830046, Peoples R China

Recommended Citation:
Zhao Wenwu,Pan Shilie,Dong Xiaoyu,et al. Synthesis, crystal structure and properties of a new lead fluoride borate, Pb3OBO3F[J]. Materials Research Bulletin,2012,47(4):947-951.
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