Synthesis, crystal structure and properties of a new lead fluoride borate, Pb3OBO3F
Zhao Wenwu; Pan Shilie; Dong Xiaoyu; Li Junjie; Tian Xuelin; Fan Xiaoyun; Chen Zhaohui; Zhang Fangfang
2012
Source PublicationMaterials Research Bulletin
ISSN0025-5408
Volume47Issue:4Pages:947-951
Abstract

A new compound, Pb3OBO3F, has been grown by the high temperature solution method from the PbO-PbF2-B2O3 system. It crystallizes in the orthorhombic system, space group Pbcm with unit-cell parameters a = 7.6313(14) angstrom, b = 6.5229(12) angstrom, c= 11.906(2) angstrom, Z = 4, volume = 592.66(19) angstrom(3). The structure of the compound is solved by the direct methods and refined to R-1 = 0.0528 and wR(2) = 0.1400. Pb3OBO3F consists of Pb(1)O3F tetrahedra, Pb(2)O-4 tetrahedra and BO3 triangles which build up the symmetrical chains extended along the c-axis. The powder X-ray diffraction pattern of the Pb3OBO3F has been measured. Functional groups presented in the sample were identified by Fourier transform infrared spectrum.

KeywordX-ray Diffraction Crystal Structure Optical Properties
Subject AreaMaterials Science
DOI10.1016/j.materresbull.2012.01.019
Indexed BySCI
WOS IDWOS:000302823800003
Citation statistics
Cited Times:14[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.xjipc.cas.cn/handle/365002/1368
Collection新疆维吾尔自治区电子信息材料与器件重点实验室
材料物理与化学研究室
Corresponding AuthorPan Shilie
Affiliation1.Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Xinjiang Key Lab Elect Informat Mat & Devices, Urumqi 830011, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China
3.Xinjiang Univ, Phys & Chem Detecting Ctr, Urumqi 830046, Peoples R China
Recommended Citation
GB/T 7714
Zhao Wenwu,Pan Shilie,Dong Xiaoyu,et al. Synthesis, crystal structure and properties of a new lead fluoride borate, Pb3OBO3F[J]. Materials Research Bulletin,2012,47(4):947-951.
APA Zhao Wenwu.,Pan Shilie.,Dong Xiaoyu.,Li Junjie.,Tian Xuelin.,...&Zhang Fangfang.(2012).Synthesis, crystal structure and properties of a new lead fluoride borate, Pb3OBO3F.Materials Research Bulletin,47(4),947-951.
MLA Zhao Wenwu,et al."Synthesis, crystal structure and properties of a new lead fluoride borate, Pb3OBO3F".Materials Research Bulletin 47.4(2012):947-951.
Files in This Item:
File Name/Size DocType Version Access License
synthesis, crystal s(561KB)期刊论文作者接受稿开放获取CC BY-NC-SAView Application Full Text
Related Services
Recommend this item
Bookmark
Usage statistics
Export to Endnote
Google Scholar
Similar articles in Google Scholar
[Zhao Wenwu]'s Articles
[Pan Shilie]'s Articles
[Dong Xiaoyu]'s Articles
Baidu academic
Similar articles in Baidu academic
[Zhao Wenwu]'s Articles
[Pan Shilie]'s Articles
[Dong Xiaoyu]'s Articles
Bing Scholar
Similar articles in Bing Scholar
[Zhao Wenwu]'s Articles
[Pan Shilie]'s Articles
[Dong Xiaoyu]'s Articles
Terms of Use
No data!
Social Bookmark/Share
File name: synthesis, crystal structure and properties of a new lead fluoride borate, pb3obo3f.pdf
Format: Adobe PDF
All comments (0)
No comment.
 

Items in the repository are protected by copyright, with all rights reserved, unless otherwise indicated.