Synthesis, crystal structure and properties of a new lead fluoride borate, Pb3OBO3F
Zhao Wenwu; Pan Shilie; Dong Xiaoyu; Li Junjie; Tian Xuelin; Fan Xiaoyun; Chen Zhaohui; Zhang Fangfang
2012
发表期刊Materials Research Bulletin
ISSN0025-5408
卷号47期号:4页码:947-951
摘要

A new compound, Pb3OBO3F, has been grown by the high temperature solution method from the PbO-PbF2-B2O3 system. It crystallizes in the orthorhombic system, space group Pbcm with unit-cell parameters a = 7.6313(14) angstrom, b = 6.5229(12) angstrom, c= 11.906(2) angstrom, Z = 4, volume = 592.66(19) angstrom(3). The structure of the compound is solved by the direct methods and refined to R-1 = 0.0528 and wR(2) = 0.1400. Pb3OBO3F consists of Pb(1)O3F tetrahedra, Pb(2)O-4 tetrahedra and BO3 triangles which build up the symmetrical chains extended along the c-axis. The powder X-ray diffraction pattern of the Pb3OBO3F has been measured. Functional groups presented in the sample were identified by Fourier transform infrared spectrum.

关键词X-ray Diffraction Crystal Structure Optical Properties
学科领域Materials Science
DOI10.1016/j.materresbull.2012.01.019
收录类别SCI
WOS记录号WOS:000302823800003
引用统计
被引频次:14[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.xjipc.cas.cn/handle/365002/1368
专题新疆维吾尔自治区电子信息材料与器件重点实验室
材料物理与化学研究室
通讯作者Pan Shilie
作者单位1.Chinese Acad Sci, Xinjiang Tech Inst Phys & Chem, Xinjiang Key Lab Elect Informat Mat & Devices, Urumqi 830011, Peoples R China
2.Chinese Acad Sci, Grad Sch, Beijing 100049, Peoples R China
3.Xinjiang Univ, Phys & Chem Detecting Ctr, Urumqi 830046, Peoples R China
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Zhao Wenwu,Pan Shilie,Dong Xiaoyu,et al. Synthesis, crystal structure and properties of a new lead fluoride borate, Pb3OBO3F[J]. Materials Research Bulletin,2012,47(4):947-951.
APA Zhao Wenwu.,Pan Shilie.,Dong Xiaoyu.,Li Junjie.,Tian Xuelin.,...&Zhang Fangfang.(2012).Synthesis, crystal structure and properties of a new lead fluoride borate, Pb3OBO3F.Materials Research Bulletin,47(4),947-951.
MLA Zhao Wenwu,et al."Synthesis, crystal structure and properties of a new lead fluoride borate, Pb3OBO3F".Materials Research Bulletin 47.4(2012):947-951.
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